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formed in the polymerization of ethylene oxide (Eq. 7-30). In fact, 1,4-dioxane is the major product in the typical polymerization of ethylene oxide (>80 90%) with only minor amounts of low molecular weight (<103) linear polymer [Kubisa, 1996; Libiszowski et al., 1989].

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The 5% rate, which was relatively low when it first formed the basis of the five per cent contracts or triple contracts discussed in an earlier chapter, now became common in Western Europe on safe deposits or special partnerships At the end of this century the Hochstetter Bank in Germany paid 5% on small deposits (283) In England the return expected by special partners may have been much higher It may have averaged in excess of 10%, (284) insofar as can be judged from imperfect evidence In Florence the State now held guardians of wards and widows responsible for a flat 5% minimum rate of return (285) The Medici Bank in Florence paid 10%, then 71 4%, and then 5% on deposits; these payments, however, were often contingent on earnings.

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Grab your tools and let s see what s inside! 1. Remove battery door and batteries. 2. Remove the two screws at the bottom of the back (these will be either Phillips or star [Torx] head). Set screws aside on your hardware magnet or some other safe place. 3. Spread case halves apart by prying with your fingers inside the battery compartment. 4. With case spread a little bit, insert a screwdriver in the lower of the four rectangular holes on the case back and gently push the plastic retaining clips to the side. The case will pop open a bit as each clip is released. 5. Do the same with the top two clips and set the back of the case in a safe place.

7-30

Cationic ROP of ethylene oxide is not useful for the synthesis of linear polymer, but is used to produce crown ethers. Propylene oxide gives less cyclic dimer than does ethylene oxide for steric reasons; cyclic tetramer predominates. The nucleophilicity of a cyclic ether relative to the ether oxygen in a polymer chain increases with ring size so that cyclic oligomer formation is somewhat less for oxetane and much less for tetrahydrofuran compared to oxirane. The cyclic tetramer is the most abundant cyclic oligomer, up to $50%, with lesser amounts of trimer and sizes from pentamer to nonamer for oxetane. No cyclic dimer is found. The cyclic oligomer fraction decreases with increasing size of substituents on the oxetane ring. For example, 3,3-bis(chloromethyl)oxirane yields linear polymer with high molecular weights (104 105 ) and no more than a few percent cyclic oligomer. The total cyclic oligomer fraction in tetrahydrofuran polymerization is less than a few percent. The cyclic tetramer is the most abundant species followed by pentamer and hexamer; only very small amounts of other-sized cyclics are formed. 7-2b-3-b Activated Monomer Polymerization. Cyclic oligomer formation can be greatly suppressed and even eliminated by carrying out cationic polymerization as an activated monomer (AM) polymerization by using an acid initiator such as BF3 or tri ic acid in the presence of an alcohol [Biedron et al., 1990; Kubisa and Penczek, 1999; Kubisa et al., 2000; Penczek et al., 1986; Wojtania et al., 1986]. Activated monomer polymerization competes with conventional cationic ROP. Initiation in conventional ROP involves the reaction of protonated monomer with unprotonated monomer (Eq. 7-31a), whereas initiation in AM ROP involves the reaction of protonated monomer with alcohol (Eq. 7-31b).

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Apache PDFBox | A Java PDF Library
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